Preview

Proceedings of Universities. Applied Chemistry and Biotechnology

Advanced search

Hydraulic tests of a random helical packing element

https://doi.org/10.21285/2227-2925-2019-9-2-320-327

Abstract

A large number of different packing elements are applied in the chemical, oil refining, petrochemical, food and other industries for implementing heat-and-mass transfer processes in columns. The advantage of packed columns consists in their high efficiency, low flow resistance and stable operation. The most important requirements for packing elements include their high specific surface area, large free volume proportion, ease of manufacture and low material consumption. However, few available packing elements meet all of the aforementioned requirements. In this work, we developed a helical packing element for implementing heat-and-mass transfer processes in distillation, absorption and extraction columns, as well as in cooling towers, and carried out a series of respective hydraulic tests. The novel packing element is characterized by a simple design, implying coiling a metal strip into a helix. Such a shape excludes the contact with neighbouring elements, which prevents blocking of the packing surface and formation of stagnant zones. A specific feature of this design consists in the smooth surface of the element, which prevents the formation of drops and streams, thus reducing the mass transfer efficiency. The film-like flow through the packing element ensures high mass transfer characteristics with minimum entrainment, thus contributing to the reduction of flow resistance. On the basis of experimental data, empirical equations were obtained for calculating the flow resistance of dry and wet packing patterns. A comparative analysis of the developed packing element with Pall Rings and Inzhekhim-2000 is provided. It is shown that the developed helical packing element is characterized by a large surface area, significant free volume and low flow resistance. In addition, the simple design of the element significantly reduces its production costs.

About the Authors

N. D. Gubanov
Irkutsk National Research Technical University
Russian Federation

Ph.D. (Engineering), Associate Professor,

Irkutsk



D. V. Medvedev
Irkutsk National Research Technical University
Russian Federation

Postgraduate Student,

Irkutsk



G. V. Bozhenkov
Irkutsk National Research Technical University
Russian Federation

Ph.D. (Chemistry), Associate Professor,

Irkutsk



References

1. Kagan A.M., Laptev A.G., Pushnov A.S., Farakhov M.I. Kontaktnye nasadki pro-myshlennykh teplomassoobmennykh apparatov [Contact nozzles of industrial heat and mass transfer apparatus]. Kazan': Otechestvo Publ., 2013, 454 p.

2. De Brito M.H., Von Stockar U., Bangerter A.M., Bomio P., Laso M. Effective Mass-Transfer Area in a Pilot Plant Column Equipped with Structured Packings and with Ceramic Rings. Industrial and Engineering Chemistry Research. 1994, vol. 33, no. 3, pp. 647–656. DOI: 10.1021/ie00027a023

3. Liu W.-Z., Wong D.S.H., Wang S.-J., Hsu H.-C. Effect of mass transfer on the design of an extractive distillation process for separating DMC and methanol. Journal of the Taiwan Institute of Chemical Engineers. 2016, vol. 60, pp. 205–212. DOI: 10.1016/j.jtice.2015.11.022

4. Hanusch F., Rehfeldt S., Klein H. Liquid Maldistribution in Random-Packed Columns: Experimental Investigation of Influencing Factors. Chemical Engineering and Technology. 2018, vol. 41, no. 11, pp. 2241–2249. DOI: 10.1002/ceat.201800467

5. Farakhov M.I., Laptev A.G., Basharov M.M. Modernization of mass-exchange equipment by new packings in chemical engineering, Theoretical Foundations of Chemical Engineering. 2015, vol. 49, issue 3, pp. 233–238. DOI: 10.1134/S0040579515030033

6. Polyanski A.V., Blinichev V.N., Chagin O.V., Kravchik Y. Estimation of the efficiency of packed mass-transfer devices. Theoretical Foundations of Chemical Engineering. 2017, vol. 51, issue 3, pp. 341–347. DOI: 10.1134/S0040579517030101

7. Danilov R.Yu., Petlyuk F.B., Serafimov L.A. Minimum-reflux regime of simple distillation columns. Theoretical Foundations of Chemical Engineering. 2007, vol. 41, issue 4, pp. 371–383. DOI: 10.1134/S0040579507040069

8. Serafimov L.A., Chelyuskina T.V., Mavletkulova P.O. Special distillation regime involving an infinite reflux ratio and an infinite number of separation stages. Theoretical Foundations of Chemical Engineering. 2014, vol. 48, issue 1, pp. 48–54. DOI: 10.1134/S0040579514010138

9. Serafimov L.A., Timoshenko A.V. Masstransfer equation in multicomponent mixtures. Theoretical Foundations of Chemical Engineering. 2005, vol. 39, issue 3, pp. 316–324. DOI: 10.1007/s11236-005-0081-9

10. Bravo J.L., Rocha J.A., Fair J.R. Mass transfer in gauze packings. Hydrocarbon Processing. 1985. vol. 64, no. 1, pp. 91–95.

11. Schmidt R. The lower capacity limits of packed columns. Institution of Chemical Engineers Symposium Series. 2017, vol. 2, no. 56, pp. 3.1/1–3.1/13.

12. Reinhard Billet. Packed towers in processing and environmental technology. New York: VCH, 1995, 382 p.

13. Bozhenkov G.V., Gubanov N.D., D'yachkova S.G., Medvedev D.V., Rudyakova E.V. Nasadka dlya teplomassoobmennykh apparatov [Nozzle for heat and mass transfer apparatus]. Patent of RF, no. 170601. 02.05.2017.

14. Farakhov T.M., Basharov M.M., Shigapov I.M. Hydraulic characteristics of new high-performance irregular heat and mass transfer nozzles. Elektronnyi nauchnyi zhurnal «Neftegazovoe delo». 2012, no. 2, pp. 192–207. (Available at: https://elibrary.ru/item.asp? id =17322447 (accessed 23.10. 2018). (In Russian)

15. Farakhov M.M., Farakhov T.M., Laptev A.G. Hydraulic characteristics of a chaotic injector for gas and liquid contact. Fundamental'nye issledovaniya. 2018, no. 3, pp. 24–28. (In Russian)

16. Ramm V.M. Absorbtsiya gazov [Gas absorption]. Moscow: Khimiya Publ., 1976, 656 p.


Review

For citations:


Gubanov N.D., Medvedev D.V., Bozhenkov G.V. Hydraulic tests of a random helical packing element. Proceedings of Universities. Applied Chemistry and Biotechnology. 2019;9(2):320-327. https://doi.org/10.21285/2227-2925-2019-9-2-320-327

Views: 550


Creative Commons License
This work is licensed under a Creative Commons Attribution 4.0 License.


ISSN 2227-2925 (Print)
ISSN 2500-1558 (Online)